The title compound—cis,exo-1,2,3,4,4a,13b-hexahydro-1,4-methano-5-isopropoxy-9H-tribenzo [b,f ]azepine—was synthesized in 83% isolated yield by a palladium-catalyzed one-pot strategy from 1-iodo-2-isopropoxybenzene and ortho-bromoaniline. The azepine derivative was fully characterized (FT-IR,MS, 1Hand 13C-NMR, elemental analysis) and all proton and carbon signals have been completely assigned by 2D NMR experiments.
Cis,exo-1,2,3,4,4a,13b-hexahydro-1,4-methano-5- isopropoxy-9H-tribenzo[b,f]azepine / Casnati, Alessandra; Motti, Elena; DELLA CA', Nicola. - In: MOLBANK. - ISSN 1422-8599. - 2018:1(2018), p. M988. [10.3390/M988]
Cis,exo-1,2,3,4,4a,13b-hexahydro-1,4-methano-5- isopropoxy-9H-tribenzo[b,f]azepine
Alessandra Casnati;Elena Motti;Nicola Della Ca’
2018-01-01
Abstract
The title compound—cis,exo-1,2,3,4,4a,13b-hexahydro-1,4-methano-5-isopropoxy-9H-tribenzo [b,f ]azepine—was synthesized in 83% isolated yield by a palladium-catalyzed one-pot strategy from 1-iodo-2-isopropoxybenzene and ortho-bromoaniline. The azepine derivative was fully characterized (FT-IR,MS, 1Hand 13C-NMR, elemental analysis) and all proton and carbon signals have been completely assigned by 2D NMR experiments.File in questo prodotto:
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