The title compound 2b was obtained as a minor product in the reaction between a thioanisole and PCl3/AlCl3. The crystal and molecular structure has been determined by single crystal X‐ray techniques. The compound crystallizes in the space group P 21/c, with α = 9.004(2), b = 13.416(3), c = 11.662(3) Å, and β = 93.1 (1)°. The molecule adoptes a “butterfly” arrangement.

A [1,2,3]Benzothiadiphospholo[3,2-b]-[1,2,3]benzothiadiphosphole as a Further Product from the Reaction of Aryl Methyl Thioethers with PCl3 and AlCl3 / G., Baccolini; C. A., Mosticchio; E., Mezzina; Rizzoli, Corrado; Sgarabotto, Paolo. - In: HETEROATOM CHEMISTRY. - ISSN 1042-7163. - 4:(1993), pp. 319-322. [10.1002/hc.520040403]

A [1,2,3]Benzothiadiphospholo[3,2-b]-[1,2,3]benzothiadiphosphole as a Further Product from the Reaction of Aryl Methyl Thioethers with PCl3 and AlCl3

RIZZOLI, Corrado;SGARABOTTO, Paolo
1993

Abstract

The title compound 2b was obtained as a minor product in the reaction between a thioanisole and PCl3/AlCl3. The crystal and molecular structure has been determined by single crystal X‐ray techniques. The compound crystallizes in the space group P 21/c, with α = 9.004(2), b = 13.416(3), c = 11.662(3) Å, and β = 93.1 (1)°. The molecule adoptes a “butterfly” arrangement.
A [1,2,3]Benzothiadiphospholo[3,2-b]-[1,2,3]benzothiadiphosphole as a Further Product from the Reaction of Aryl Methyl Thioethers with PCl3 and AlCl3 / G., Baccolini; C. A., Mosticchio; E., Mezzina; Rizzoli, Corrado; Sgarabotto, Paolo. - In: HETEROATOM CHEMISTRY. - ISSN 1042-7163. - 4:(1993), pp. 319-322. [10.1002/hc.520040403]
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Utilizza questo identificativo per citare o creare un link a questo documento: https://hdl.handle.net/11381/2313532
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