γ-CuCl microcrystals were found to segregate in self-assembled (CnH2n+1NH3)2CuCl4 hybrid organic-inorganic films deposited by single source thermal ablation. The microcrystals dispersed in the hybrid have sizes of 35 nm, as estimated from X-ray diffraction patterns. The UV photoluminescence efficiency of the embedded microcrystals is more than 100 times higher than that of CuCl films having similar crystallite sizes.
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